Volume 10, number 1

Synthesis, Analytical, Spectral and X-ray Diffraction Studies of Cu(II)andNi(II) Complexes with Glipizide, 1-Cyclohexyl3 [[p [2(5methylpyrazinecarboxamido)ethyl]phenyl]sulfonyl]urea, An Oral Antidiabetic Agent

Neeti Rathore1 and Balkrishan2

1Department of Chemistry, Saifia Science College, Bhopal - 462001, India.

2Department of Chemistry, Gyan Ganga College

 

DOI : http://dx.doi.org/10.13005/bbra/1157

ABSTRACT: Complexes of transition metals like Cu(II) and Ni(II) with Glipizide1cyclohexyl 3[[p[2(5methyl pyrazine carboxamido) ethyl] phenyl] Sulphonyl] urea were synthesized. Metalcomplexes were characterized byelemental analysis, IR and NMR.The crystal structure of complexeswasdetermined by X-ray diffraction method. The XRD data was used to calculate various parameters like crystal system, volume, density, porosity, particle size etc.based on these studiestetrahedral geometry has been proposed for these complexes.

KEYWORDS: Glipizide; Crystal structure; metal complex; IR; NMR; XRD

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Rathore N, Balkrishan. Synthesis, Analytical, Spectral and X-ray Diffraction Studies of Cu(II)andNi(II) Complexes with Glipizide, 1-Cyclohexyl3 [[p [2(5methylpyrazinecarboxamido)ethyl]phenyl]sulfonyl]urea, An Oral Antidiabetic Agent. Biosci Biotechnol Res Asia 2013;10(1)
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Rathore N, Balkrishan. Synthesis, Analytical, Spectral and X-ray Diffraction Studies of Cu(II)andNi(II) Complexes with Glipizide, 1-Cyclohexyl3 [[p [2(5methylpyrazinecarboxamido)ethyl]phenyl]sulfonyl]urea, An Oral Antidiabetic Agent. Biosci Biotechnol Res Asia 2013;10(1). Available from: https://www.biotech-asia.org/?p=10552

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